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Controllable Synthesis of CoMoOx Nanostructures for High Energy Density Asymmetric Supercapacitors

ZENG Xiaojun, DING Junqing, ZHANG Zuliang, ZHANG Xiaoye, SUN Liangliang

(Advanced Ceramic Materials Research Institute, School of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen 333403, Jiangxi, China)

Abstract: Supercapacitors exhibit high power density and long-term cycle life time in energy-power applications. Multi-component metal oxides are promising electrode materials for supercapacitors, due to their multivalent cations and diverse charge/discharge kinetics. However, it is difficult to control the morphology of multi-component metal oxides and the regulation methodsareusually too complicated. In this work, CoMoOx nanostructures were grown on the surface of nickel foam by using a simple one-step hydrothermal method. The controllable synthesis of Co0Mo1Ox ultra-thin nanosheets, Co1Mo2Ox interwoven nanosheets, Co1Mo1Ox nanoflowers and Co2Mo1Ox nanopillar structures was realized by adjusting the Co:Mo molar ratio. Among them, the unique structure of Co1Mo1Ox nanoflowers enabled high specific capacitance and excellent cycling stability, with a specific capacitance of as high as 1628.8 F•g−1 at a current density of 5 A•g−1, which is superior to numerous advanced Co/Mo-based electrode materials. The Co1Mo1Ox nanoflowers can still retain 93.5% of the specific capacitance after 2000 cycles of galvanostatic charge-discharge (GCD) cycling. In addition, asymmetric supercapacitors (ASCs) devices assembled with Co1Mo1Ox nanoflowers and activated carbon (AC) exhibited high energy density, delivering an energy density of 79.3 Wh•kg−1 at a power density of 4 kW•kg−1. This work provides a controllable synthesis strategy of multi-component metal oxide nanostructures and enriches self-supporting, binder-free, and high energy storage properties of electrode materials for pseudocapacitors.

Key words: CoMoOx nanostructures; controllable synthesis; high energy density; pseudocapacitor; asymmetric supercapacitors

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